Metrohm 930 Compact IC Flex Oven/SeS/Deg User Manual Page 6
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- Table of contents
- TROUBLESHOOTING
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Table of contents
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭
IV
￭￭￭￭￭￭￭￭
930 Compact IC Flex Oven/SeS/Deg (2.930.2460)
3.13 Metrohm CO
2
Suppressor (MCS) ....................................... 36
3.13.1 General information on MCS ................................................. 36
3.13.2 Connecting the MCS ............................................................. 37
3.13.3 Installing adsorption cartridges .............................................. 38
3.14 Installing the detector ........................................................ 40
3.15 Connecting the sample degasser (optional) ..................... 40
3.16 Connecting the instrument to a computer ....................... 42
3.17 Connecting the instrument to the power supply ............. 43
3.18 Initial start-up ..................................................................... 44
3.19 Connecting and rinsing the guard column ....................... 46
3.20 Connecting the separation column ................................... 48
3.21 Conditioning ........................................................................ 51
4 Operation 53
5 Operation and maintenance 54
5.1 IC system ............................................................................. 54
5.1.1 Operation .............................................................................. 54
5.1.2 Care ...................................................................................... 54
5.1.3 Maintenance by Metrohm Service .......................................... 54
5.1.4 Shutting down and starting back up ...................................... 55
5.2 Capillary connections ......................................................... 56
5.3 Servicing the door .............................................................. 56
5.4 Column oven – replacing the capillaries ........................... 56
5.5 Handling the eluent ............................................................ 58
5.5.1 Manufacturing eluent ............................................................ 58
5.5.2 Changing the eluent .............................................................. 59
5.6 Servicing the eluent degasser ........................................... 59
5.7 Notes on operating the high-pressure pump ................... 60
5.8 Servicing the high-pressure pump .................................... 61
5.9 Servicing the inline filter .................................................... 74
5.10 Servicing the pulsation absorber ...................................... 77
5.11 Injection valve ..................................................................... 77
5.12 Suppressor .......................................................................... 77
5.12.1 Notes for operating the suppressor ........................................ 77
5.12.2 Taking care of the suppressor housing ................................... 78
5.12.3 Servicing the suppressor ........................................................ 78
5.13 Servicing the Metrohm CO
2
Suppressor (MCS) ................ 85
5.13.1 Replacing the CO
2
adsorption cartridge ................................. 85
5.13.2 Regenerating the H
2
O adsorption cartridge ............................ 85
- 930 Compact IC Flex 1
- Table of contents 5
- 4 Operation 53 6
- 6 Troubleshooting 90 7
- 8 Warranty (guarantee) 100 7
- 9 Accessories 102 7
- Index 104 7
- Table of figures 8
- 1 Introduction 9
- ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 10
- ￭￭￭￭￭￭￭￭ 10
- 1.2 Intended use 11
- 1.3 Safety instructions 11
- 1.3.2 Electrical safety 12
- 1.3.5 Recycling and disposal 13
- 1.4 Symbols and conventions 14
- 2 Overview of the instrument 15
- 2.2 Rear 16
- 2 Overview of the instrument 17
- ￭ Openings on the door 18
- ￭ Openings on the back panel 18
- 3 Installation 21
- ￭ Hex key 4 mm (6.2621.030) 24
- 3.5 Column oven 27
- 3 Installation 33
- 3.11 Injection valve 34
- 3.12 Suppressor 36
- 3.13 Metrohm CO 44
- 3.13.2 Connecting the MCS 45
- 3.14 Installing the detector 48
- 3.18 Initial start-up 52
- 3.21 Conditioning 59
- 4 Operation 61
- 5 Operation and maintenance 62
- 5.2 Capillary connections 64
- 5.3 Servicing the door 64
- Figure 15 Column oven 65
- 5.5 Handling the eluent 66
- 5.5.2 Changing the eluent 67
- 5 Operation and maintenance 69
- 5.11 Injection valve 85
- 5.12 Suppressor 85
- 5.12 Suppressor 86
- 5.14 Servicing the detector 94
- 5.15 Rinsing the sample path 94
- 5.16 Separation column 95
- 6 Troubleshooting 98
- 6 Troubleshooting 101
- 7 Technical specifications 102
- 7.4 Housing 103
- 7.5 Leak sensor 103
- 7.6 Column oven 103
- 7.8 High-pressure pump 104
- 7.7 Eluent degasser 104
- 7.9 Injection valve 105
- 7.10 Suppressor 105
- 7.11 Metrohm CO 105
- Suppressor (MCS) 105
- 7.12 Detector 106
- 7.13 Sample degasser 106
- 7.14 Power connection 106
- 7.15 Interfaces 106
- 7.16 Safety specifications 107
- 8 Warranty (guarantee) 108
- 9 Accessories 110
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