Metrohm 850 Professional IC AnCat MCS User Manual Page 47
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- Table of contents
- TROUBLESHOOTING
- BOOKMARKS
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2 Installation
850 Professional IC – AnCat – MCS
￭￭￭￭￭￭￭￭
37
4
Setting the flow rate
￭ Start MagIC Net (if not yet started).
￭ Ensure that the eluent aspiration tubing is immersed sufficiently in
the eluent.
￭ Let the high pressure pump run.
5
Aspirating eluent
￭ Aspirate with the syringe (19-1) until bubble-free eluent flows into
the syringe.
6
Completing deaerating
￭ Turn off high pressure pump.
￭ Close rotary knob (19-7).
￭ Remove syringe (19-1) from the Luer connector (19-2).
￭ Pull the purging needle (19-3) out of the deaerating capillary
(19-4).
2.11 Inline filter
Between the purge valve and the pulsation damper the 6.2821.120 inline
filter is installed as protection against particles.
Inline filters protect the separation column securely against possible con-
tamination from the eluent. Inline filters can however also just as well be
used for the purpose of protecting the suppressor against contaminations
in the regeneration or rinsing solutions. The fine 2 µm material of the
readily and easily replaceable filter platelets removes particles such as bac-
teria and algae from the solutions.
Note
The inline filter is already installed in the newly delivered instrument.
The following installation instructions need not be carried out at the
time of initial installation.
- 850 Professional IC 1
- Table of contents 5
- 3 Start-up 66 6
- 5 Troubleshooting 100 7
- 8 Accessories 116 8
- Index 131 8
- Table of figures 9
- ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 10
- ￭￭￭￭￭￭￭￭ 10
- 1 Introduction 11
- 1.1 Instrument description 12
- 1 Introduction 13
- 1.2 Intended use 15
- 1.3 About the documentation 15
- 1.4 Safety instructions 16
- 1.4.5 Recycling and disposal 18
- 2 Installation 19
- 2.3 Flow diagram 21
- Regeneration solution 22
- Rinsing solution 22
- Sample optional 22
- 2 Installation 23
- 2.4.1 Packaging 24
- 2.4.2 Checks 24
- 2.4.3 Location 24
- 2.6 Rear of the instrument 26
- 2.6 Rear of the instrument 28
- Detector 1 29
- Detector 2 29
- 2.6.4 Leak sensor 31
- 2.6.5 Drainage tubing 32
- Figure 8 Drainage tubing 33
- 2) and (8-4) 33
- 2.8 Eluent 37
- 2.8 Eluent 38
- 2.9 Eluent degasser 41
- 2.10 High pressure pump 42
- 2.10 High pressure pump 44
- 2.11 Inline filter 47
- 2.12 Pulsation damper 48
- 2.13 Sample degasser 50
- 2.14 Injection valve 51
- 2.14 Injection valve 52
- 2.15 Column thermostat 54
- Figure 25 Column thermostat 55
- 2.16.2 Connecting the MSM 57
- 2.17 Peristaltic pump 60
- 2.17 Peristaltic pump 62
- 2.18 Metrohm CO 65
- 2.19 Conductivity detector 68
- 2.19 Conductivity detector 70
- 2.21 Guard column 72
- 2.22 Separation column 74
- 3 Start-up 76
- 3.2 Conditioning 77
- 4 Operation and maintenance 79
- 4.2 Capillary connections 80
- 4.3 Door 81
- 4.4 Eluent 81
- 4.5 High pressure pump 82
- 4.5.2 Maintenance 83
- 4.5 High pressure pump 84
- 4.6 Inline filter 93
- 4.8 Rinsing the sample path 95
- 4.9 Sample degasser 97
- 4.10 Injection valve 97
- 4.11.3 Maintenance 98
- 4.12 Peristaltic pump 103
- 4.12.2 Maintenance 104
- 4 Operation and maintenance 105
- 4.13 Metrohm CO 106
- suppressor (MCS) 106
- 4.15 Separation column 107
- 4.14 Conductivity detector 107
- 4.15.2 Protection 108
- 4.15.3 Storage 108
- 4.15.4 Regeneration 108
- 5 Troubleshooting 110
- 5 Troubleshooting 111
- 6 Technical specifications 115
- 6.5 Housing 116
- 6.6 Eluent degasser 116
- 6.7 High pressure pump 116
- 6.8 Sample degasser 117
- 6.9 Injection valve 117
- 6.10 Column thermostat 118
- 6.12 Peristaltic pump 118
- 6.13 Metrohm CO 119
- 6.15 Mains connection 120
- 6.16 Interfaces 120
- 6.17 Safety specification 121
- 6.19 Weight 121
- 7 Conformity and warranty 122
- 7.3 Warranty (guarantee) 124
- 8 Accessories 126
- 8 Accessories 127
- 8.1 Scope of delivery 128
- 8.2 Optional accessories 137
- 8.2 Optional accessories 138
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