Metrohm 850 Professional IC AnCat MCS User Manual Page 41
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- Table of contents
- TROUBLESHOOTING
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2 Installation
850 Professional IC – AnCat – MCS
￭￭￭￭￭￭￭￭
31
5
Eluent
6
Aspiration filter 6.2821.090
7
Filter holder
From accessory set 6.2744.210.
8
Clamping screw
From accessory set 6.2744.210.
9
Tubing weighting
From accessory set 6.2744.210.
10
Eluent bottle 6.1608.070
11
Bottle attachment 6.1602.160
12
SGJ clip 6.2023.020
13
Tubing nipple
14
Thread stopper
2.9 Eluent degasser
Gas bubbles in the eluent lead to an unstable baseline, as high pressure
pumps can transport liquids, but not gases. The eluent therefore has to be
degassed, before it reaches the high pressure pump.
The eluent degasser removes gas bubbles and dissolved gases from the
eluent. For degassing, the eluent flows into a vacuum chamber through a
special fluoropolymer capillary.
Note
The eluent degasser is already installed in the newly delivered instru-
ment. The following installation instructions need not be carried out at
the time of initial installation.
Connecting the eluent degasser
5
6
1
2
3
4
Figure 16
Eluent degasser
1
Eluent degasser input
2
Eluent degasser output
- 850 Professional IC 1
- Table of contents 5
- 3 Start-up 66 6
- 5 Troubleshooting 100 7
- 8 Accessories 116 8
- Index 131 8
- Table of figures 9
- ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 10
- ￭￭￭￭￭￭￭￭ 10
- 1 Introduction 11
- 1.1 Instrument description 12
- 1 Introduction 13
- 1.2 Intended use 15
- 1.3 About the documentation 15
- 1.4 Safety instructions 16
- 1.4.5 Recycling and disposal 18
- 2 Installation 19
- 2.3 Flow diagram 21
- Regeneration solution 22
- Rinsing solution 22
- Sample optional 22
- 2 Installation 23
- 2.4.1 Packaging 24
- 2.4.2 Checks 24
- 2.4.3 Location 24
- 2.6 Rear of the instrument 26
- 2.6 Rear of the instrument 28
- Detector 1 29
- Detector 2 29
- 2.6.4 Leak sensor 31
- 2.6.5 Drainage tubing 32
- Figure 8 Drainage tubing 33
- 2) and (8-4) 33
- 2.8 Eluent 37
- 2.8 Eluent 38
- 2.9 Eluent degasser 41
- 2.10 High pressure pump 42
- 2.10 High pressure pump 44
- 2.11 Inline filter 47
- 2.12 Pulsation damper 48
- 2.13 Sample degasser 50
- 2.14 Injection valve 51
- 2.14 Injection valve 52
- 2.15 Column thermostat 54
- Figure 25 Column thermostat 55
- 2.16.2 Connecting the MSM 57
- 2.17 Peristaltic pump 60
- 2.17 Peristaltic pump 62
- 2.18 Metrohm CO 65
- 2.19 Conductivity detector 68
- 2.19 Conductivity detector 70
- 2.21 Guard column 72
- 2.22 Separation column 74
- 3 Start-up 76
- 3.2 Conditioning 77
- 4 Operation and maintenance 79
- 4.2 Capillary connections 80
- 4.3 Door 81
- 4.4 Eluent 81
- 4.5 High pressure pump 82
- 4.5.2 Maintenance 83
- 4.5 High pressure pump 84
- 4.6 Inline filter 93
- 4.8 Rinsing the sample path 95
- 4.9 Sample degasser 97
- 4.10 Injection valve 97
- 4.11.3 Maintenance 98
- 4.12 Peristaltic pump 103
- 4.12.2 Maintenance 104
- 4 Operation and maintenance 105
- 4.13 Metrohm CO 106
- suppressor (MCS) 106
- 4.15 Separation column 107
- 4.14 Conductivity detector 107
- 4.15.2 Protection 108
- 4.15.3 Storage 108
- 4.15.4 Regeneration 108
- 5 Troubleshooting 110
- 5 Troubleshooting 111
- 6 Technical specifications 115
- 6.5 Housing 116
- 6.6 Eluent degasser 116
- 6.7 High pressure pump 116
- 6.8 Sample degasser 117
- 6.9 Injection valve 117
- 6.10 Column thermostat 118
- 6.12 Peristaltic pump 118
- 6.13 Metrohm CO 119
- 6.15 Mains connection 120
- 6.16 Interfaces 120
- 6.17 Safety specification 121
- 6.19 Weight 121
- 7 Conformity and warranty 122
- 7.3 Warranty (guarantee) 124
- 8 Accessories 126
- 8 Accessories 127
- 8.1 Scope of delivery 128
- 8.2 Optional accessories 137
- 8.2 Optional accessories 138
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