Metrohm 792 Basic IC User Manual Page 51
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2 Installation
792 Basic IC
42
4 Check for leaks
x
Check all capillaries and their connections between the high-
pressure pump and the detector block for escaping liquid. If
eluent escapes anywhere, the appropriate compression fitting
must be tightened further or changed.
5 Condition system
x
Rinse the system with eluent until the desired stability of the
baseline is reached (normally 30
}
60 min; if the eluent is
changed, the establishment of the ion exchanger equilibrium
on the separating column can take longer).
x
The instrument is now ready for sample determinations using
the selected system.
2.9.2 Putting into operation with suppressor
Before sample solutions can be injected at the
792
Basic IC
(with use
of the suppressor), the entire system must be tested for leaks and then
conditioned with eluent until the baseline is stable. At the same time,
the suppressor module must be conditioned. Proceed as follows:
1 Open system "Prep MSM.smt"
x
Start the
«
792 Basic IC
»
PC program, if it has not already
been started (see
section 2.5.3
).
x
Select
File / Open / System
in the main window. Open the folder
Suppressed anion
and select the system file
Prep MSM.smt
.
Click on
<Open>
.
2 Open control window
x
Double-click the 792 icon in the system window. The control
window for manual control of the 792 Basic IC appears, which
indicates conductivity, pressure and current system parame-
ters.
- BasicBasic 1
- Table of contents 2
- Notes – Maintenance – Faults 5
- Appendix 6
- List of figures 7
- 1 Introduction 10
- 1 Introduction 15
- 1.733.0110 Detector block) 15
- 1.3.1 Organization 17
- SYSTEM STATE 18
- <OK> 18
- 1.4 Safety notes 19
- 2 Installation 20
- 2.2.1 Packaging 22
- 2.2.2 Check 22
- 2.2.3 Location 22
- 2.3.5 Filter unit PEEK 25
- 2.4 Mains connection 26
- 2.4.2 Fuses 27
- 2.5 Connection to the PC 28
- 2.5.3 Basic settings 29
- Hardware 31
- Hardware settings 31
- Cell constant 31
- 2.6 High-pressure pump 32
- File / Open / System 34
- Default.smt 34
- <Open> 34
- 2 mL/min 35
- <Send to unit> 35
- Injector 38
- Flow rate 39
- <On> 39
- <Off> 39
- 2.8 Suppressor module 44
- 2.9 Putting into operation 50
- Suppressed anion 51
- Prep MSM.smt 51
- Startup determination 52
- 2 Installation 53
- 3 Operating tutorial 54
- 3.2 Preparations 55
- 3.3 Calibration 56
- <Concentrations> 61
- <Calibrate> 61
- 3.4 Sample determination 63
- 4 Operation 66
- 4.1.2 Glossary 67
- 4.1.4 Main window elements 69
- 4.1.9 Help 72
- 4.2.1 Fonts 73
- 4.2.2 Security system 73
- 4.2.3 Global settings 74
- 4.2.4 COM port 76
- 4.3 Systems 77
- 4.3.3 System functions 78
- 4.3.4 PC icon 80
- 4.3.5 Watch window 80
- 4.3.6 Instrument icon 81
- 4.3.7 System state window 87
- 4.3 Systems 88
- Error messages 88
- 4.4 Methods 89
- Data Log 95
- <Add new> 95
- New comment 95
- 4.4.3 Method setup 96
- 4.4.4 Integration 99
- 792 Basic IC 100
- 792 Basic IC 101
- Component table 103
- Components table 105
- 4.4.6 Report output 115
- 4.5 Chromatograms 127
- 4.5.4 Peak editor 136
- 4.5.5 Printing 138
- 4.6 Batch reprocessing 141
- REPROCESS / 145
- <Merge> 145
- Appearance 145
- File / Save / Chroma 145
- 5.1.1 Separating columns 148
- 5.1.2 High-pressure pump 149
- 5.1.3 Eluents 150
- 5.1.4 Peristaltic pump 150
- 5.1.5 Suppressor module 151
- 5.1.6 Connections 151
- 5.2.1 General information 152
- 5.2.2 Passivation 152
- 5.2.3 Recycling 153
- 5.2.4 Shutdown 153
- 90 and 158
- 5.3 Faults and malfunctions 165
- 6 Appendix 168
- 6.1.3 Injection valve 169
- 6.1.4 High-pressure pump 169
- 6.1.5 Peristaltic pump 170
- 6.1.6 Suppressor module 170
- 6.1.7 RS232 interface 170
- 6.1.8 Mains connection 171
- 6.1.9 Safety specifications 171
- 6.1.11 Ambient temperature 172
- 6.1.12 Housing 172
- 6.2 Standard equipment 173
- 6.3 Optional accessories 176
- 6.3 Optional accessories 178
- 6 Appendix 179
- 6.4 Warranty and conformity 185
- EU Declaration of Conformity 186
- 6.5 Index 188
- 6.5 Index 190
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