Metrohm 873 Biodiesel Rancimat Manual User Manual

873 Biodiesel RancimatManual8.873.8003EN

1.2 Rancimat method￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭873 Biodiesel Rancimata GLP test set to carry out these tests (see Optional accessories, page180).1.

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭92￭￭￭￭￭￭￭￭873 Biodiesel RancimatFormula 2 for stability timeResult of the calculation with formula 2.Formula 3 for st

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭93Cell constantCell constant of the conductivity measuring cell used to record the dete

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭94￭￭￭￭￭￭￭￭873 Biodiesel Rancimat[Best Fit]Adjust the column width to the longest field content (including title).Grid

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭95PreviewDisplay of the selected format for the cells.FontSelection of the font type fr

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭96￭￭￭￭￭￭￭￭873 Biodiesel RancimatSizeFont size in points for the selected font type.SelectionFont sizeFind WhatRequire

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭97Match caseon | off (Default value: off)If this option is activated, the search is onl

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭98￭￭￭￭￭￭￭￭873 Biodiesel RancimatCriteriaCriteria for filtering data sets.orFurther criteria for filtering data sets.I

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭994.7.2 Determination and method dataFor each determination you can view all the deter

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭100￭￭￭￭￭￭￭￭873 Biodiesel RancimatID 1Sample identification 1.ID 2Sample identification 2.Determination dateDate and t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭101Induction time automaticAutomatically determined induction time.Induction time manua

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction873 Biodiesel Rancimat￭￭￭￭￭￭￭￭3MeasuringvesselConductivitymeasuring cellMeasuringsolutionReaction vesselSampleHeat

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭102￭￭￭￭￭￭￭￭873 Biodiesel RancimatMethod nameName of the method.Creation dateDate when the method was last saved.Creat

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭103Delta TTemperature correction: indication of how much the block temperature hasbeen

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭104￭￭￭￭￭￭￭￭873 Biodiesel RancimatEvaluate induction timeThe induction time has been automatically determined (see &qu

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭105Formula 1 for induction timeThe automatically determined induction time was calculat

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭106￭￭￭￭￭￭￭￭873 Biodiesel RancimatFormula parametersFactorParameter for the calculation of the standard time. It indic

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭107Report elementsHeaderOutput of the header.CurveOutput of the curves.Method descripti

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭108￭￭￭￭￭￭￭￭873 Biodiesel RancimatDirectoryDirectory in which the report has been saved.DescriptionThe following warni

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭109Single graph, multiple graph or live graphProceed as follows to open a single graph

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭110￭￭￭￭￭￭￭￭873 Biodiesel Rancimat￭ Click on the symbol or the menu item Determina-tion ▶ Graphics ▶ Live graph with

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭111Copying graphs and pasting them into other programsProceed as follows to copy a grap

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭873 Biodiesel Rancimat[Next] Button or keyWarningThis symbol draws attention to a possible life

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭112￭￭￭￭￭￭￭￭873 Biodiesel RancimatSetting the stability time manuallyIn order to set the stability time manually, you

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭113 3Set second tangent￭ Keep the [Shift] key and left mouse button pressed down toset

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭114￭￭￭￭￭￭￭￭873 Biodiesel RancimatExtrapolation of several resultsProceed as follows to carry out an extrapolation of

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭115 3Update the display￭ Click on the [Update] button.The graph and all results are upd

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭116￭￭￭￭￭￭￭￭873 Biodiesel RancimatPrinting extrapolation resultsSee "Printing extrapolation results", page 1

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭117r2Calculated correlation coefficient. If this value is below the limit value (see&qu

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭118￭￭￭￭￭￭￭￭873 Biodiesel RancimatThe dialog window Recalculation appears. 2Adjust the parameters￭ Activate the option

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭119NoteA detailed description of the parameters can be found at "Recalcu-late stab

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭120￭￭￭￭￭￭￭￭873 Biodiesel Rancimat￭ Click on the tab Standards. 2Adjust the parameters￭ Activate the options Recalcula

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭121Evaluation delayWaiting time until starting the curve evaluation.Evaluation suppress

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction873 Biodiesel Rancimat￭￭￭￭￭￭￭￭5Flammable substancesWarningThe oven of the 873 Biodiesel Rancimat can be heated to

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭122￭￭￭￭￭￭￭￭873 Biodiesel RancimatRecalculate formula 1 for induction timeon | off (Default value: off)Activate/Deacti

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭123Calculation activeon | off (Default value: off)If this option is activated, the para

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭124￭￭￭￭￭￭￭￭873 Biodiesel Rancimat4.7.6 Printing and exporting dataPrinting results from the Control windowProceed as

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭125￭ Click on the option Overview table and/or Overview list.NoteIn the overview table,

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭126￭￭￭￭￭￭￭￭873 Biodiesel RancimatPrinting graphsProceed as follows to print a single graph, multiple graph or live gr

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭127Printing the report defined under "Settings"Proceed as follows to print th

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭128￭￭￭￭￭￭￭￭873 Biodiesel Rancimat 2Print extrapolation results￭ Click on the symbol or the menu item File ▶ Print...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭129 3Export data￭ Click on the symbol or the menu item Determina-tion ▶ Export ▶ Deter

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭130￭￭￭￭￭￭￭￭873 Biodiesel Rancimat￭ Click on [Yes] to delete the exported determination in the originaldatabase.Openin

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭131 2Select determination￭ Select the determination of which the data is to be exported

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭873 Biodiesel RancimatMains voltageWarningAn incorrect mains voltage can damage the instrument.O

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭132￭￭￭￭￭￭￭￭873 Biodiesel RancimatDefinition of elements for report outputHeaderon | off (Default value: on)Output of

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭133with offseton | off (Default value: off)If this option is activated, the curves are

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭134￭￭￭￭￭￭￭￭873 Biodiesel Rancimat"Results" tabOn the Results tab, you can carry out the settings for the re

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭135Acc. to methodAxis scaling in accordance with the settings defined in the method und

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭136￭￭￭￭￭￭￭￭873 Biodiesel RancimatInduction timeThe induction time is used for extrapolation. If the induction time ha

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭137Retain zoom at determination changeon | off (Default value: off)The selected zoom ra

4.8 GLP functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭138￭￭￭￭￭￭￭￭873 Biodiesel Rancimat4.8 GLP functions4.8.1 General information on GLP and validationGLP (Good La

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭139The dialog window GLP properties for unit with serial no. xappears. 2Switch on monit

4.8 GLP functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭140￭￭￭￭￭￭￭￭873 Biodiesel RancimatToleranceIndication of the tolerance value for the relevant GLP test. If the r

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭1414.8.4 Carrying out GLP tests4.8.4.1 TemperatureFor the GLP test for temperature me

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument873 Biodiesel Rancimat￭￭￭￭￭￭￭￭72 Overview of the instrument873Biodiesel Rancimat1110987654321Figure

4.8 GLP functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭142￭￭￭￭￭￭￭￭873 Biodiesel Rancimat 2Screw on accessories￭ Use the hexagon key to lightly tighten the hexagon scr

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭143 2Enter calibration points of the temperature sensor￭ Click on the menu item Tools ▶

4.8 GLP functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭144￭￭￭￭￭￭￭￭873 Biodiesel RancimatThe following dialog window appears: 4Insert GLP test set and start measuremen

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭145 5Carry out measurement for further channelsWarningThe aluminum cylinder of the GLP

4.8 GLP functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭146￭￭￭￭￭￭￭￭873 Biodiesel Rancimat4.8.4.2 ConductivityThe GLP test for conductivity measurement can be carried

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭147 2Carry out GLP test with test resistor￭ Click on the menu item Tools ▶ GLP test ▶ C

4.8 GLP functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭148￭￭￭￭￭￭￭￭873 Biodiesel Rancimat￭ Click on the menu item Tools ▶ GLP test ▶ Conductivity... andconfirm with [N

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭149 4Confirm or reject results✓Test passed: The deviation of the measured conductivitie

4.8 GLP functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭150￭￭￭￭￭￭￭￭873 Biodiesel Rancimat￭ Click on the menu item Tools ▶ GLP test ▶ Gas flow... and con-firm with [Nex

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭151 3Confirm or reject results✓Test passed: The deviation of the measured gas flow valu

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭873 Biodiesel Rancimat11Reaction vessel (6.1429.040)Molecular sieve flaskFilterAir out2Air/N inPt 100RS 232WARNING - F

4.8 GLP functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭152￭￭￭￭￭￭￭￭873 Biodiesel RancimatProceed as follows to print out a test identification: 1Print GLP certificate￭

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭153 2Display detailed results￭ Double click on the required GLP test within the fields

4.8 GLP functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭154￭￭￭￭￭￭￭￭873 Biodiesel Rancimat￭ Select the Serial number of the required instrument and confirmwith [OK].The

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Handling and maintenance873 Biodiesel Rancimat￭￭￭￭￭￭￭￭1555 Handling and maintenance5.1 General information5.1.1 CareThe 873

5.3 Regenerating or replacing the molecular sieve￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭156￭￭￭￭￭￭￭￭873 Biodiesel Rancimat5.3 Regenerating or replacing the molecular s

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Handling and maintenance873 Biodiesel Rancimat￭￭￭￭￭￭￭￭157Display Cause RemedyDeviceBUSY test error. Switch the instrument offa

5.5 Quality Management and validation with Metrohm￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭158￭￭￭￭￭￭￭￭873 Biodiesel RancimatNoteYou can find information on the subjects

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting873 Biodiesel Rancimat￭￭￭￭￭￭￭￭1596 Troubleshooting6.1 ProblemsProblem Cause RemedyThe pump is louderthan norm

6.1 Problems￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭160￭￭￭￭￭￭￭￭873 Biodiesel RancimatProblem Cause RemedyNo air flow can bedetected in the measur-ing vessel (it does no

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting873 Biodiesel Rancimat￭￭￭￭￭￭￭￭161Problem Cause RemedyThe induction times arenot reproducible formultiple determ

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument873 Biodiesel Rancimat￭￭￭￭￭￭￭￭913FEP tubing 250 mm (6.1805.080)For supplying the air from the intern

6.1 Problems￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭162￭￭￭￭￭￭￭￭873 Biodiesel RancimatProblem Cause RemedyThe conductivity measuringcell is contaminated.Check measuring

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting873 Biodiesel Rancimat￭￭￭￭￭￭￭￭163Problem Cause RemedyDuring the measurement,sample evaporates in the reac-tion

6.1 Problems￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭164￭￭￭￭￭￭￭￭873 Biodiesel RancimatProblem Cause RemedyThe curve progression is tooflat with the result that auto-mati

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications873 Biodiesel Rancimat￭￭￭￭￭￭￭￭1657 Technical specifications7.1 General dataNumber of instru-ments th

7.3 Conductivity measurement￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭166￭￭￭￭￭￭￭￭873 Biodiesel RancimatShutdown temper-ature260 ± 11 °C(if this temperature is exceeded, t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications873 Biodiesel Rancimat￭￭￭￭￭￭￭￭1677.5 GLP test setExternal tempera-ture sensorTypePt100 casing element

7.8 Safety specification￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭168￭￭￭￭￭￭￭￭873 Biodiesel Rancimat7.8 Safety specificationDesign and testingAccording to EN/IEC/UL 61010

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications873 Biodiesel Rancimat￭￭￭￭￭￭￭￭1697.11 HousingCover materialPolyurethane hard foam (PUR) with flame re

8.1 Declaration of Conformity￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭170￭￭￭￭￭￭￭￭873 Biodiesel Rancimat8 Conformity and warranty8.1 Declaration of ConformityThis is to

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty873 Biodiesel Rancimat￭￭￭￭￭￭￭￭171Metrohm Ltd. is holder of the SQS certificate ISO 9001:2000 Quality ma

3.1 Setting up the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭873 Biodiesel Rancimat3 Installation3.1 Setting up the instrument3.1.1 PackagingThe in

8.3 Warranty (guarantee)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭172￭￭￭￭￭￭￭￭873 Biodiesel RancimatManufactureThe measures put into practice in the production of our inst

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories873 Biodiesel Rancimat￭￭￭￭￭￭￭￭1739 AccessoriesNoteSubject to change without notice.9.1 Scope of delivery 2.873.00

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭174￭￭￭￭￭￭￭￭873 Biodiesel RancimatQty. Order no. Description1 6.1429.050 Reaction vessel long for stability

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories873 Biodiesel Rancimat￭￭￭￭￭￭￭￭175Qty. Order no. Description1 6.1608.050 Drying bottle / 100 mL / GL 45Material: Cle

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭176￭￭￭￭￭￭￭￭873 Biodiesel RancimatQty. Order no. Description1 6.1808.020 Tubing adapter olive / M6 inner1 M6

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories873 Biodiesel Rancimat￭￭￭￭￭￭￭￭177Qty. Order no. Description8 6.1819.080 Cannula for gas feedingFor stability measur

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭178￭￭￭￭￭￭￭￭873 Biodiesel RancimatQty. Order no. Description1 6.2134.100 RS-232 cable 5 m, 9-pin - 9-pinConn

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories873 Biodiesel Rancimat￭￭￭￭￭￭￭￭179Qty. Order no. Description1 6.2724.010 Dust filterDust filter for Rancimats and Ka

9.2 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭180￭￭￭￭￭￭￭￭873 Biodiesel RancimatQty. Order no. DescriptionUSA, …: Type NEMA/ASA6.2122.0701 8.873.8003EN

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories873 Biodiesel Rancimat￭￭￭￭￭￭￭￭181Order no. Description6.2301.060 KCl ion standard 250 mLKCl ion standard (250 mL, c

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭11Molecular sieve flaskFilterAir out2Air/N inFromflaskToflask89101211123654 7Figure

9.2 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭182￭￭￭￭￭￭￭￭873 Biodiesel RancimatOrder no. Description6.5616.010 GLP Test SetGLP test set for the exact

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Index873 Biodiesel Rancimat￭￭￭￭￭￭￭￭183IndexAAccessoriesMount ... 10Access rightsAdjust ...

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭184￭￭￭￭￭￭￭￭873 Biodiesel RancimatMeasuring vesselEquip ... 13Method ...

3.2 Mounting accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭873 Biodiesel Rancimat 2Mount drying flaskCautionDo not fill the hot molecular sieve directly

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭133.2.2 Mounting accessories for the external air supplyIf the laboratory air is he

3.2 Mounting accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭873 Biodiesel Rancimat2134567891020161211131415171819Figure 5 Equipping the reaction and measu

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭1515Connector plug16Measuring vessel cover (6.0913.130)Contains integrated conductiv

3.2 Mounting accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭873 Biodiesel Rancimat3.2.4 Inserting vessels / Establishing tubing connectionsAfter you have

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭17Proceed as follows to mount the collection tube: 1Mount the exhaust collection tub

3.3 Mains connection￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭873 Biodiesel Rancimat3.3.2 Replacing fusesTwo fuses 4 A (slow-acting) for 115 V or 2 A (slow-act

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭19WarningAny interruption to the grounding within or outside the instrument canmake

3.4 Connecting a PC￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭873 Biodiesel RancimatMemory approx. 20 MB for program filesRS-232 interface one free RS-232 interf

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭213.4.2.3 Windows VistaCautionIf you run the software 873 Biodiesel Rancimat on a c

Metrohm AGCH-9101 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] Biodiesel RancimatManual8.873.8003EN

3.4 Connecting a PC￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭873 Biodiesel Rancimat 3Set Administrator password￭ Do not enter a password, instead click on [OK].

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭23Establishing the device communication 1Follow the instructions in Section 4.2.1.

4.1 Fundamentals of operation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭873 Biodiesel Rancimat4 OperationThis section describes the most important points for op

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭254.1.2 TermsControl window The main window 873 Biodiesel RancimatControl is called th

4.1 Fundamentals of operation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭873 Biodiesel RancimatAn image of the Biodiesel Rancimat is shown in the Control panel, w

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭27Options Carry out general settings, set instrument config-uration, manage access righ

4.1 Fundamentals of operation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭873 Biodiesel RancimatOpening and closing the Results windowProceed as follows to open an

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭29In the Results window subwindows with a determination overview, single,multiple or li

4.1 Fundamentals of operation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭873 Biodiesel RancimatSpecial filterDefine filter (see Chapter 4.7.1, page 83).Apply filt

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭31*.mel Event fileThis file contains a protocol of all events whichhave occurred with t

TeachwareMetrohm AGCH-9101 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

4.1 Fundamentals of operation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭873 Biodiesel Rancimat 3Switch zoom off again￭ Right click in the graphs window.The conte

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭334.2 Instrument and Program Settings4.2.1 Establishing the instrument communicationU

4.2 Instrument and Program Settings￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭873 Biodiesel Rancimat￭ If a softswitch is used, activate the option Softswitch in

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭35After having entered the access rights, the Login window for selecting theuser and en

4.2 Instrument and Program Settings￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭873 Biodiesel Rancimat 3Activate/Deactivate the rights￭ Click on the symbol to op

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭37Deleting a userProceed as follows to delete an existing user: 1Open Users and groups

4.2 Instrument and Program Settings￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭873 Biodiesel RancimatStarting heating block A once automaticallyProceed as follows

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭39 2Set automatic start time￭ Under Start heating select the option Daily.￭ Click on th

4.2 Instrument and Program Settings￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭873 Biodiesel RancimatDisplaying the gas flowProceed as follows: 1Open dialog windo

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭41Switching the temperature log on and offProceed as follows: 1Switch on the recording

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents873 Biodiesel Rancimat￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 Instrument description ...

4.3 Program information￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭873 Biodiesel RancimatOptimizing the databaseProceed as follows to optimize the standard databa

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭43 2Print instrument information￭ Click on the button [Print report…].The status report

4.3 Program information￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭873 Biodiesel RancimatNoteThe block Service diagnosis is password-protected and only accessible

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭45Sample ID1Sample identification 1.StatusStatus of the channel.ready: No active measur

4.3 Program information￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭46￭￭￭￭￭￭￭￭873 Biodiesel RancimatNoteYou can find the meaning of the symbols and columns in the eventoverv

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭47￭ Click on the symbol or the menu item Filter ▶ Selection basedfilter.Only entries

4.4 Calibration functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭48￭￭￭￭￭￭￭￭873 Biodiesel RancimatTimeTime of the event. The format depends on the settings defined in Wi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭49 2Enter cell constants￭ Enter the cell constants of the conductivity measuring cells

4.4 Calibration functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭50￭￭￭￭￭￭￭￭873 Biodiesel Rancimat￭ Enter the conductivity of the standard used.c(KCl) = 1 mmol/L can be

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭51134567892910Figure 6 Equipping the reaction vessel for determining Delta T1FEP tubing

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭873 Biodiesel Rancimat4.1.6 Context-sensitive menus ...

4.4 Calibration functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭52￭￭￭￭￭￭￭￭873 Biodiesel RancimatPreparing Delta T determinationFigure 6 shows in detail how the accesso

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭53￭ Click on the symbol .The dialog window with the method parameters is opened.￭ Unde

4.4 Calibration functions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭54￭￭￭￭￭￭￭￭873 Biodiesel RancimatNoteYou can find the calibration data (T1 to T3) for Metrohm sensors on

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭55NoteIf the temperature which is defined in the method, has not yet beenreached, the h

4.5 Methods￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭56￭￭￭￭￭￭￭￭873 Biodiesel Rancimat 2Adjust parameters￭ Adjust the required parameters.￭ Click on the tab Evaluation and

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭57Opening a selected method and adjusting parametersProceed as follows to open the meth

4.5 Methods￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭58￭￭￭￭￭￭￭￭873 Biodiesel RancimatNoteA method which is still selected in one of the blocks A or B, cannot berenamed. S

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭59 2Save it with a new name￭ If necessary, adjust the parameters (see Chapter 4.5.2, pa

4.5 Methods￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭60￭￭￭￭￭￭￭￭873 Biodiesel RancimatPrinting parameters of a methodProceed as follows to print the parameters of an exist

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭61TemperatureSetpoint temperature of the sample.Range50 ... 220 °CDelta TTemperature co

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents873 Biodiesel Rancimat￭￭￭￭￭￭￭￭V5 Handling and maintenance 1555.1 General information ...

4.5 Methods￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭62￭￭￭￭￭￭￭￭873 Biodiesel RancimatTable 1 Approximate values for determining Delta TSetpoint temperature Delta T80 °C90

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭63per blockThe 4 channels of a block can be started and stopped jointly.Stop criteriaTi

4.5 Methods￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭64￭￭￭￭￭￭￭￭873 Biodiesel RancimatTime Conductivity Endpoint(s) Analysis stops... ✔ ✔after reaching the first criterion

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭65Evaluate induction timeon | off (Default value: on)Determination of the induction tim

4.5 Methods￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭66￭￭￭￭￭￭￭￭873 Biodiesel RancimatRange0 ... 100 hEvaluation suppressionStartTime from the start of the determination t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭672nd derivativeTimeConductivityInduction timeEndStartEvaluationsuppressionEvaluationde

4.5 Methods￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭68￭￭￭￭￭￭￭￭873 Biodiesel RancimatTime axis (x)SelectionAuto scaling | Manual scalingAuto scalingAutomatic definition o

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭694.5.2.4 "Formulas" tabYou can enter values for further automatic calculati

4.5 Methods￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭70￭￭￭￭￭￭￭￭873 Biodiesel RancimatFormula 3 for stability time:on | off (Default value: off)If this option is switched

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭71FactorParameter for the calculation of the standard time, which indicates the factorb

Table of figures￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VI￭￭￭￭￭￭￭￭873 Biodiesel RancimatTable of figuresFigure 1 Measuring arrangement (schematic representation) ...

4.5 Methods￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭72￭￭￭￭￭￭￭￭873 Biodiesel RancimatMethod parameterson | off (Default value: on)Output of the method parameters.Curve(s)

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭73Example of an automatically printed reportGLP test passed.10.02.2007 09:34:03Printing

4.5 Methods￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭74￭￭￭￭￭￭￭￭873 Biodiesel Rancimat4.5.2.7 "Description" tabYou can enter a comment on the method in this tab

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭754.6 DeterminationsStandard sequence Optional steps Further informationPrepare instru

4.6 Determinations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭76￭￭￭￭￭￭￭￭873 Biodiesel Rancimat4.6.1 Preparing the instrument and the accessoriesThe cleanliness of instrume

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭77 4Weigh in the sampleNoteUse new reaction vessels and air tubes for each measurement.

4.6 Determinations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭78￭￭￭￭￭￭￭￭873 Biodiesel RancimatNoteDifferent methods with different temperatures can be selected forBlock A a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭79 4Insert and connect reaction vesselsNoteThe temperature defined in the method must b

4.6 Determinations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭80￭￭￭￭￭￭￭￭873 Biodiesel RancimatThe determination is automatically saved in the databaseRepos.mrd. The channel

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭81￭ Then heat the Iso-Versinic® tubings in the drying oven for 2 hoursat 80 °C.4.6.5 A

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction873 Biodiesel Rancimat￭￭￭￭￭￭￭￭11 Introduction1.1 Instrument descriptionThe 873 Biodiesel Rancimat is a PC-contro

4.6 Determinations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭82￭￭￭￭￭￭￭￭873 Biodiesel Rancimat 2Save measured data and results￭ Confirm the message with [Yes] to save all d

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭834.7 Results4.7.1 Determination overviewThe determination overview displays selected

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭84￭￭￭￭￭￭￭￭873 Biodiesel RancimatA detailed description of the parameters can be found at "Parameterdescription&q

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭85￭ Position the cursor in the title line of the table between two col-umns.The cursor

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭86￭￭￭￭￭￭￭￭873 Biodiesel Rancimat 4Change the font￭ Click on the menu item Format ▶ Fonts...The following dialog wind

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭87￭ Click on the upper left in the title line.Searching for determinationsProceed as fo

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭88￭￭￭￭￭￭￭￭873 Biodiesel RancimatDisplaying or hiding selected determinationsProceed as follows to display or hide pre

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭89Filtering determinations with the special filterWith a special filter you can define

4.7 Results￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭90￭￭￭￭￭￭￭￭873 Biodiesel Rancimat 3Specify the filter criteria￭ In the column determination date in field Criteria ent

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation873 Biodiesel Rancimat￭￭￭￭￭￭￭￭91Printing and exporting the determination overviewSee Chapter 4.7.6, Page 124.Paramete