Metrohm 940 Professional IC Vario ONE/SeS/Prep 2 User Manual

940 Professional IC Vario940 Professional IC Vario ONE/SeS/Prep 2Manual – Short Instructions8.940.8114EN

2.1 Instrument description￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)2 Introduction2.1 Instrument descripti

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Introduction940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭3Leak sensorThe leak sensor detects leaking liquid th

2.2 Intended use￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)Metrohm CO2 Suppressor (MCS)The Metrohm CO2 Suppre

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Introduction940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭5The present instrument is suitable for processing ch

2.3 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)Mains voltageWARNINGAn incorrect mains volt

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Introduction940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭72.3.5 Recycling and disposalThis product is covered

2.4 Symbols and conventions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)NOTEThis symbol highlights additional i

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Overview of the instrument940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭93 Overview of the instrument3.1 Fron

3.1 Front￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)5Suppressor6Column thermostatWith two column holders for

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Overview of the instrument940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭113.2 RearFigure 2 Rear1Bottle holderO

3.2 Rear￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)5Vacuum connectionFor connecting an Extension Module that

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭134 Installation4.1 Setting up the instrument4.1.1

4.3 Removing transport locking screws￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)Removing the handle4.3 Remo

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭15Remove the transport locking screwsFigure 3 Removin

4.4 Connecting the drainage tubing and leak sensor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)4.4 Connecting

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭17Connecting the drainage tubing4.4.2 Connecting the

4.5 Column thermostat￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)4.5 Column thermostatThe column thermostat

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭19Connecting the eluent aspiration tubing

4.7 Connecting the eluent degasser￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)4.7 Connecting the eluent dega

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭21NOTEThe instruments are supplied without rotor and

Metrohm AGCH-9100 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] Professional IC Vario940 Professional

4.12 Suppressor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)Inserting large rotorsInserting small rotorsYou ne

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭23Figure 4 Suppressor – connection capillaries1outOut

4.12 Suppressor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)Alternative installationInstalling bottles with au

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭254.13 Metrohm CO2 Suppressor (MCS)4.13.1 Connectin

4.13 Metrohm CO2 Suppressor (MCS)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)CO2 adsorption cartridge, an H2O

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭274.14 Installing the detectorThe 940 Professional I

4.15 Connecting the sample degasser (optional)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)4.15 Connecting th

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭294.16 Peristaltic pump4.16.1 Installing the perist

4.16 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)Setting the contact pressure correctly 1￭ Fu

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭314.17 Installing the 6-port valveDuring sample prep

TeachwareMetrohm AGCH-9100 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

4.19 Connecting the instrument to the power supply￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)Connecting the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭33Connecting the power supply cable 1Inserting the po

4.20 Initial start-up￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)Rinsing the IC systemCAUTIONThe guard column

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭35 4Deaerating the high-pressure pump Use the syringe

4.21 Connecting and rinsing the guard column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)4.21 Connecting and

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭37￭ Start manual control in MagIC Net and select the

4.22 Connecting the separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420) Rinse the separation column

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Installation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭39￭ Rinse the separation column with eluent for appro

4.23 Conditioning￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭ Visually inspect whether all capillaries and t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭415 OperationThe 940 Professional IC Vario – ONE/SeS/Pr

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭IIITable of contents1 About these Short Instructio

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)6 Warranty (guarantee)Metrohm guarantees that the deliveries and

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Warranty (guarantee)940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭43The same warranty periods that are specifie

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)7 AccessoriesUp-to-date information on the scope of delivery and

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Accessories940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭45The Partslists webpage will be displayed. 7Select th

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭46￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)IndexNumbers/Symbols6-port valve ...

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)4.13 Metrohm CO2 Suppressor (MCS) ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of figures940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭VTable of figuresFigure 1 Front ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 About these Short Instructions940 Professional IC Vario ONE/SeS/Prep 2 (2.940.1420)￭￭￭￭￭￭￭￭11 About these Short InstructionsT