Metrohm 832 KF Thermoprep User Manual

CH-9101 Herisau/Switzerland E-Mail [email protected] Internet www.metrohm.com 832 KF Thermoprep Instructions for Use

2.1 General 6 832 KF Thermoprep, Safety information 2 Safety information Warning! This instrument should only be used in accordance with the

2.2 Electrical safety 832 KF Thermoprep, Installation 7 3 Installation This section describes the things you should pay attention to when un-pac

3.1 Instrument setup 8 832 KF Thermoprep, Installation 3.1 Instrument setup 3.1.1 Packaging The 832 KF Thermoprep and its specially packed access

3.2 Mains connection 832 KF Thermoprep, Installation 9 • Pull out mains cable Remove the mains cable from the mains supply connection of the 83

3.3 Assembling the 832 KF Thermoprep 10 832 KF Thermoprep, Installation 3.3 Assembling the 832 KF Thermoprep 3.3.1 Assembling the needles Fig.

3.3 Assembling the 832 KF Thermoprep 832 KF Thermoprep, Installation 11 3.3.2 Attaching the drying bottles 1. Fill 6.1608.050 drying bottles 15

3.4 Assembling the coulometric cell 12 832 KF Thermoprep, Installation 3.4 Assembling the coulometric cell Fig. 9 Coulometer cell The coulome

4.1 Inserting and removing sample vials 832 KF Thermoprep, Operation 13 4 Operation This section describes the basic principles of handling the

4.3 The pump 14 832 KF Thermoprep, Operation Loosen the red clamping lever by pressing it strongly and lower the guide head and needle by using b

4.4 The temperature controller 832 KF Thermoprep, Operation 15 4.4 The temperature controller The best proven dTron 16.1 (JUMO) temperature con

II 832 KF Thermoprep Teachware Metrohm AG Oberdorfstr. 68 CH-9101 Herisau [email protected] These instructions are protected by cop

4.4 The temperature controller 16 832 KF Thermoprep, Operation 4.4.3 Self-optimization of the control parameters Self-optimization should only be

4.5 Working procedure 832 KF Thermoprep, Operation 17 4.5 Working procedure Warning! As both the sample vials and the oven become very hot the

4.5 Working procedure 18 832 KF Thermoprep, Operation 4.5.1 Preparing the 832 KF Thermoprep/756/831 Coulometer system 1. Switch on the 832 KF Th

4.5 Working procedure 832 KF Thermoprep, Operation 19 5. Raise the needle fully and remove the blank sample vial from the oven with the crimpin

4.6 Practical information 20 832 KF Thermoprep, Operation 4.6 Practical information Selecting the carrier gas Nitrogen (N2) should be used as th

4.6 Practical information 832 KF Thermoprep, Maintenance information 21 5 Maintenance information The 832 KF Thermoprep does not need a lot of c

7.1 Problems 22 832 KF Thermoprep, Troubleshooting 7 Troubleshooting 7.1 Problems Problem Possible cause Remedy Molecular sieve in the drying b

8.1 Technical data 832 KF Thermoprep, Annex 23 8 Annex In this section you will find the most important technical data of the 832 KF Thermoprep,

8.1 Technical data 24 832 KF Thermoprep, Annex 8.1.6 Electromagnetic compatibility (EMC) Emission Standards fulfilled: - EN/IEC 61326-1 - EN 550

8.2 Standard equipment 832 KF Thermoprep, Annex 25 8.2 Standard equipment Immediately upon receipt of the instrument please check that the deliv

832 KF Thermoprep III Table of contents 1 Introduction 1 1.1 Description of the instrument ...

8.2 Standard equipment 26 832 KF Thermoprep, Annex 2 6.1821.040 Inlet tube for drying bottle, with filter, L=92 mm 1 6.2049.030 Spacer with

8.3 Optional accessories 832 KF Thermoprep, Annex 27 8.3 Optional accessories 8.3.1 Sample vials Order no. Description 6.2419.000 Sample vials

8.4 Warranty and conformity 28 832 KF Thermoprep, Annex 8.4 Warranty and conformity 8.4.1 Warranty The warranty on our products is limited to de

8.4 Warranty and conformity 832 KF Thermoprep, Annex 29 8.4.2 EU Declaration of Conformity for 832 KF Thermoprep EU Declaration of Conformity

8.4 Warranty and conformity 30 832 KF Thermoprep, Annex 8.4.3 Declaration of Conformity Certificate of Conformity and System Validation This is

Index 832 KF Thermoprep, Index 31 Index <ENTER> ...19 <START>...18, 19 A Accessorie

Index 32 832 KF Thermoprep, Index SOP ...21 Spacer ...10 Standard accessori

IV 832 KF Thermoprep 7 Troubleshooting 22 7.1 Problems ...

1.1 Description of the instrument 832 KF Thermoprep, Introduction 1 1 Introduction Thanks to its reliability and simple handling, the Metrohm 83

1.2 Information about these Instructions for Use 2 832 KF Thermoprep, Introduction 1.2 Information about these Instructions for Use Please read

1.3 Parts and controls 832 KF Thermoprep, Introduction 3 1.3 Parts and controls 1.3.1 Individual parts and standard accessories Fig. 1 Fron

1.3 Parts and controls 4 832 KF Thermoprep, Introduction 1.3.2 Rear view Vorsicht: Heis se Gehäuseteile (über 60°C)Attention

1.3 Parts and controls 832 KF Thermoprep, Introduction 5 1.3.3 Temperature controller Fig. 3 Temperature controller 31 Actual value display