Metrohm 814 USB Sample Processor User Manual

814 USB Sample ProcessorManual8.814.8001EN

1.2 Instrument description￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭814 USB Sample ProcessorUp to three control devices (Titrandos, Dosing Interfaces, USB Sample

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction814 USB Sample Processor￭￭￭￭￭￭￭￭32.814.00101-Tower version￭ 1 membrane pumpe and 1 valve￭ 1 connector for an exter

1.2 Instrument description￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭814 USB Sample Processor2.814.01202-Tower version￭ 4 membrane pumps and 4 valves￭ 2 stirrer c

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction814 USB Sample Processor￭￭￭￭￭￭￭￭51.2.3 Intended useThe 814 USB Sample Processor is designed for usage as an autom

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭814 USB Sample ProcessorWarningThis symbol draws attention to a possible biologicalhazard.Cautio

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction814 USB Sample Processor￭￭￭￭￭￭￭￭7Mains voltageWarningAn incorrect mains voltage can damage the instrument.Only ope

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭814 USB Sample ProcessorWarningAlways install the safety shield supplied with the equipment befo

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction814 USB Sample Processor￭￭￭￭￭￭￭￭91.4.5 Flammable solvents and chemicalsWarningAll relevant safety measures are to

2.1 Front and rear￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭814 USB Sample Processor2 Overview of the instrument2.1 Front and rear1234567Figure 2 Front 814 US

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument814 USB Sample Processor￭￭￭￭￭￭￭￭11USB 212345678T1T2Figure 3 Rear 814 USB Sample Processor1Distributo

2.2 Rear panel￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭814 USB Sample Processor2.2 Rear panelUSB 2USB 1Contr.MSB 1MSB 2MSB 3Made by MetrohmHerisau Switzerland

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument814 USB Sample Processor￭￭￭￭￭￭￭￭13Magnet codesEvery single sample rack can be unambiguously identifi

3.1 Setting up the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭814 USB Sample Processor3 Installation3.1 Setting up the instrument3.1.1 PackagingThe

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation814 USB Sample Processor￭￭￭￭￭￭￭￭153.3 Connecting a computer The 814 USB Sample Processor requires a USB connectio

3.4 Installing rinsing and aspiration equipment￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭814 USB Sample ProcessorFor Windows Vista: The instrument is recognized

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation814 USB Sample Processor￭￭￭￭￭￭￭￭176.1805.5106.1805.4206.1808.1706.1812.0001234Figure 8 Mounting the rinsing and as

3.4 Installing rinsing and aspiration equipment￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭814 USB Sample ProcessorNoteThe opening of the tubing may need to be wi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation814 USB Sample Processor￭￭￭￭￭￭￭￭19 3Fix the rinsing tubings￭ Place the rinsing tubings into the guide chain.3.5 G

3.6 Installing the titration head￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭814 USB Sample ProcessorCautionTake care to ensure when mounting tubing and cables th

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation814 USB Sample Processor￭￭￭￭￭￭￭￭216.0xxx.xxx6.1236.0206.2740.0206.2709.0706.1543.2006.1543.170111224356Figure 12 I

Metrohm AGCH-9101 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] USB Sample ProcessorManual8.814.8001E

3.6 Installing the titration head￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭814 USB Sample Processor 6Connect a electrode cable to the electrode.Connecting the t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation814 USB Sample Processor￭￭￭￭￭￭￭￭23Connecting the tower stirrerA DIN socket for connecting a rod stirrer (802 Stirr

3.6 Installing the titration head￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭814 USB Sample ProcessorInsert the rod stirrer802 Stirrer6.1906.01012Figure 17 Insert

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation814 USB Sample Processor￭￭￭￭￭￭￭￭25The magnetic stirrer can be moved sideways as needed.3.7 Connecting an external

3.8 Connecting MSB devices￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭814 USB Sample Processor3.8 Connecting MSB devicesIn order to connect MSB devices, e.g.sti

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation814 USB Sample Processor￭￭￭￭￭￭￭￭273.8.1 Connecting dosing devicesThree dosing devices can be connected to the ins

3.8 Connecting MSB devices￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭814 USB Sample Processor3.8.2 Connecting a stirrer or titration standYou can use a magneti

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation814 USB Sample Processor￭￭￭￭￭￭￭￭293.8.3 Connecting a remote boxInstruments that are controlled via remote lines a

3.9 Connecting USB devices￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭814 USB Sample Processor3.9 Connecting USB devicesTwo USB connectors (Type A sockets) are a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation814 USB Sample Processor￭￭￭￭￭￭￭￭31Switch the barcode reader to programming mode and make the followingsettings: 1￭

TeachwareMetrohm AGCH-9101 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

3.11 Attaching the sample rack￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭814 USB Sample Processor3.11 Attaching the sample rack1Figure 25 Attaching the rackPut

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation814 USB Sample Processor￭￭￭￭￭￭￭￭33123Figure 26 Mount the safety shieldProceed as follows: 1Loosen the knurled scre

4.1 General￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭814 USB Sample Processor4 Handling and maintenance4.1 GeneralThe 814 USB Sample Processor requires approp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Troubleshooting814 USB Sample Processor￭￭￭￭￭￭￭￭355 Troubleshooting5.1 Sample ProcessorProblem Cause RemedyThe instrument isn

6.1 Beaker sensor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭814 USB Sample Processor6 Appendix6.1 Beaker sensorEvery tower of a Sample Processor is equipped wi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Appendix814 USB Sample Processor￭￭￭￭￭￭￭￭37Figure 28 Spray nozzles - FunctioningThe height of the nozzles can be adjusted in th

6.3 Remote interface￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭814 USB Sample Processor6.3.1 Pin assignment of the remote interface13114251131425Figure 30 Pin a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Appendix814 USB Sample Processor￭￭￭￭￭￭￭￭39Assigment Pin No. Assigment Pin No.Input 6 24 Output 6 1Input 7 12 Output 7 20 volts

7.1 Lift and turntable￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭814 USB Sample Processor7 Technical specifications7.1 Lift and turntableStroke path235 mmMaxim

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications814 USB Sample Processor￭￭￭￭￭￭￭￭417.4 Mains connectionVoltage100…240 VFrequency50…60 HzPower consump-

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents814 USB Sample Processor￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 The 814 USB Sample Processor in the T

7.7 Ambient temperature￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭814 USB Sample Processor7.7 Ambient temperatureNominal functionrange5…45 °CHumidity < 80 %S

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty814 USB Sample Processor￭￭￭￭￭￭￭￭438 Conformity and warranty8.1 Declaration of ConformityThis is to ce

8.2 Warranty (guarantee)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭814 USB Sample ProcessorEN 61010-2-081 Particular requirements for automatic and semi-automati

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty814 USB Sample Processor￭￭￭￭￭￭￭￭458.3 Quality Management PrinciplesMetrohm Ltd. holds the ISO 9001:200

8.3 Quality Management Principles￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭46￭￭￭￭￭￭￭￭814 USB Sample Processortional Qualification and Performance Verification of the syst

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭479 AccessoriesNoteSubject to change without notice.9.1 Scope of delivery 814 USB

9.1 Scope of delivery 814 USB Sample Processor 2.814.0010￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭48￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description3 6.1446.01

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭49Qty. Order no. Description3 6.1805.420 FEP tubing / M6 / 48 cmWith light and kink

9.1 Scope of delivery 814 USB Sample Processor 2.814.0010￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭50￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description1 6.2621.03

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭51Qty. Order no. Description3 6.2740.020 Spray nozzleFor the fine-spraying of the r

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭814 USB Sample Processor3.9 Connecting USB devices ...

9.2 Scope of delivery 814 USB Sample Processor 2.814.0020￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭52￭￭￭￭￭￭￭￭814 USB Sample Processor9.2 Scope of delivery 814 USB Sample

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭53Qty. Order no. Description1 6.1446.160 Thermometer stopper, B-14/15, obliqueinser

9.2 Scope of delivery 814 USB Sample Processor 2.814.0020￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭54￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description1 6.1805.11

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9.2 Scope of delivery 814 USB Sample Processor 2.814.0020￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭56￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description1 6.2151.00

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭57Qty. Order no. Description3 6.2709.070 Guiding sleeveFor fixation of buret and do

9.3 Scope of delivery 814 USB Sample Processor 2.814.0030￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭58￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description6.2122.0701

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭59Qty. Order no. Description1 6.2621.030 Hexagon key 4 mmLength (mm): 731 6.2621.07

9.4 Scope of delivery 814 USB Sample Processor 2.814.0110￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭60￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description1 6.2751.08

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭61Qty. Order no. Description4 6.1236.020 Sleeve with SGJ 14/12 mmSleeve with SGJ 14

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents814 USB Sample Processor￭￭￭￭￭￭￭￭V9 Accessories 479.1 Scope of delivery 814 USB Sample Processor2.814.0010 ...

9.4 Scope of delivery 814 USB Sample Processor 2.814.0110￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭62￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description2 6.1805.11

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭63Qty. Order no. Description2 6.2053.000 Cable clipCable clip for fastening cables

9.4 Scope of delivery 814 USB Sample Processor 2.814.0110￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭64￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description1 6.2621.14

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭65Qty. Order no. Description4 T.240.0102 Ferrite coresAnti-interference adapters1 6

9.5 Scope of delivery 814 USB Sample Processor 2.814.0120￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭66￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description10 6.1446.0

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭67Qty. Order no. Description4 6.1621.000 Container 10 LAs rinsing or waste containe

9.5 Scope of delivery 814 USB Sample Processor 2.814.0120￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭68￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description2 6.1805.51

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭69Qty. Order no. Description2 6.2042.020 Buret tip clip (magnetic stirrer)Clip for

9.5 Scope of delivery 814 USB Sample Processor 2.814.0120￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭70￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description1 6.2621.14

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭71Qty. Order no. Description4 T.240.0102 Ferrite coresAnti-interference adapters1 6

Table of figures￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VI￭￭￭￭￭￭￭￭814 USB Sample ProcessorTable of figuresFigure 1 The Titrando system ...

9.6 Scope of delivery 814 USB Sample Processor 2.814.0130￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭72￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description2 6.1805.11

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭73Qty. Order no. Description1 6.2621.140 Hexagon key 2.5 mm6 6.2709.070 Guiding sle

9.7 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭74￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description1 8.814.8001EN 814 USB Sample Processor Manu

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭75Qty. Order no. Description1 2.802.0020 802 StirrerRod stirrer for sample changer

9.7 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭76￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description1 2.843.0150 843 Pump Station (peristaltic)

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭77Qty. Order no. Description1 6.1458.030 KF titration head with 4 x M10 threadWith

9.7 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭78￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description1 6.2041.320 Sample rack 16 x 150 mLSample r

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭79Qty. Order no. Description1 6.2041.460 Sample rack 21 x 100 mL (COD)Sample rack 2

9.7 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭80￭￭￭￭￭￭￭￭814 USB Sample ProcessorQty. Order no. Description1 6.2711.060 Drip pan for 730/778/814/838Dri

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories814 USB Sample Processor￭￭￭￭￭￭￭￭81Qty. Order no. DescriptionCFR Part 11 as well as GLP. Dialogue languages: German,

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction814 USB Sample Processor￭￭￭￭￭￭￭￭11 Introduction1.1 The 814 USB Sample Processor in the Titrando sys-temThe 814 U

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭82￭￭￭￭￭￭￭￭814 USB Sample ProcessorIndexNumbers/Symbols685 Dosimat ....... 27700 Dosino .....