Metrohm MVA-21 User Manual download pdf

Application Bulletin 403/1 e

Installation instruction for MVA-21:

894 Professional CVS fully automated for CVS determinations

The «MVA-21» is a fully automated system for the

determination of suppressor and brightener in plating

solutions.

• PC controlled operation.

• Manual operations:

o Filling of the sample vials on the Sample

Processor with suppressor standard solution,

plating bath samples and rinsing solution.

• Automatic addition of 4 solutions: VMS, brightener

concentrate, suppressor concentrate and suppressor

standard or plating bath sample.

• Automatic rinsing of the measuring vessel.

• Method change during the determination series is

possible.

• Applications:

o Analysis of suppressor concentration in plating

baths with CVS.

o Analysis of brightener concentration in plating

baths with CVS.

Fig 1 MVA-21

Content

1. Instruments and accessories .......................................... 2

2. System setup .................................................................. 2

2.1. Electrical connections ......................................... 2

2.2. Tubing connections for rinsing and draining of the

measuring vessel ................................................ 3

2.3. Tubing connections for automatic dosing of

standard solutions and auxiliary solutions ........... 4

3. viva Configuration ........................................................... 5

3.1. Devices – 894 Profesional CVS .......................... 5

3.2. Sensors/Electrodes ............................................. 5

3.3. Dosing units ........................................................ 5

3.4. Solutions ............................................................. 6

3.5. Devices – 858 Professional Sample Processor for

CVS ..................................................................... 6

3.6. Needle adjustment .............................................. 7

4. viva «Method» ................................................................ 8

4.1. Method run .......................................................... 8

4.2. Evaluation ........................................................... 9

5. Operation...................................................................... 10

5.1. Suppressor determination series ...................... 10

5.2. Brightener determination series ........................ 11

6. Remarks ....................................................................... 12

6.1. Single additive setup ......................................... 12

6.2. Combination of applications .............................. 12

6.3. Storing dosing units........................................... 12

6.4. Storing electrodes ............................................. 12

6.5. Waste container ................................................ 12

Page 1 of 12

1 2 3 4 5 6 ... 11 12

Summary of Contents

Page 1 - Content

Application Bulletin 403/1 e Installation instruction for MVA-21: 894 Professional CVS fully automated for CVS determinations The «MVA-21» is a ful

Page 2 - 2. System setup

Application Bulletin 403/1 e Installation instruction for MVA-21 4.2.4. Results In the «Results» part on the tab «Results» the substance is select

Page 3

Application Bulletin 403/1 e Installation instruction for MVA-21 5.2. Brightener determination series 5.2.1. Manual operation • Dosing Unit «89

Page 4

Application Bulletin 403/1 e Installation instruction for MVA-21 6. Remarks 6.1. Single additive setup If the system is only used for suppressor o

Page 5 - 3. viva Configuration

Application Bulletin 403/1 e Installation instruction for MVA-21 1. Instruments and accessories Quantity Article number 1 2.894.1210 894 Prof

Page 6 - TANDARD SOLUTION

Application Bulletin 403/1 e Installation instruction for MVA-21 2.2. Tubing connections for rinsing and draining of the measuring vessel Fig 3:

Page 7

Application Bulletin 403/1 e Installation instruction for MVA-21 2.3. Tubing connections for automatic dosing of standard solutions and auxiliary

Page 8 - 4. viva «Method»

Application Bulletin 403/1 e Installation instruction for MVA-21 Fig 8: Detailed view for the tubing connections of the dosing unit waste port 3.

Page 9 - – GO TO RINSING POSITION

Application Bulletin 403/1 e Installation instruction for MVA-21 Dosing rate port 1 Maximum mL/L Dosing rate port 2 Maximum mL/L Dosing rate Fi

Page 10 - 5. Operation

Application Bulletin 403/1 e Installation instruction for MVA-21 Swing head Swing position 0 mm Rinse position 0 mm External position Not used

Page 11 - AMPLE has to be selected

Application Bulletin 403/1 e Installation instruction for MVA-21 9. Once the needle is properly adjusted select the tab «Assign position». 10. Th

Page 12 - 6. Remarks

Application Bulletin 403/1 e Installation instruction for MVA-21 4.1.5. Rinsing measuring vessel After each sample the measuring vessel need to be

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Metrohm MVA-21 User Manual

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