Metrohm 930 Compact IC Flex Oven/SeS/PP/Deg User Manual

930 Compact IC Flex930 Compact IC Flex Oven/SeS/PP/DegManual8.930.8020EN

5.12 Suppressor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭90￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭ The rotor's sealing surface is approximately 4 m

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭915.13 Peristaltic pump5.13.1 Notes on oper

5.13 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭92￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)5.13.2.2 Replacing the filterThe filters inserte

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭935.14 Servicing the Metrohm CO2 Suppressor

5.15 Servicing the detector￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭94￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560) 2Regenerating the adsorber materialAllow t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭95The time upon stopping the watch correspond

5.17 Separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭96￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)representative) or on the Internet at http://www

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭975.18 Quality Management and qualification

6.1 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭98￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)6 TroubleshootingProblem Cause RemedyMarked drop inpressure.Leak

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭99Problem Cause RemedySuppressor blocked. ￭ Regenerate

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭11 Introduction1.1 Instrument descriptionThe 930 Compact

6.1 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭100￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Problem Cause RemedyPeristaltic pump – Filterblocked.Replace the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭101Problem Cause RemedyThe eluent contains gasbubbles.￭

6.1 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭102￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Problem Cause RemedyVacuum is not beingbuiltEluent degasser – Vac

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭1037 Technical specifications7.1 Reference c

7.4 Housing￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭104￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)7.4 HousingDimensionsWidth 302 mmHeight 562 mmDepth 368 m

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭1057.7 Eluent degasserMaterial FluoropolymerR

7.9 Injection valve￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭106￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)7.9 Injection valveActuator switch-ing timetyp. 1

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭1077.13 DetectorYou can find the technical sp

7.17 Safety specifications￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭108￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)7.17 Safety specificationsThis instrument

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Warranty (guarantee)930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭1098 Warranty (guarantee)Metrohm guarantees that

1.1 Instrument description￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)High-pressure pumpThe intelligent and low-pul

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭110￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)The same warranty periods that are specified for a corresponding newp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭1119 AccessoriesUp-to-date information on the scope of del

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭112￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)The Partslists webpage will be displayed. 7Select the desired output

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Index930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭113IndexAAdsorption cartridgesConnection ... 4

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭114￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)MMains voltage ... 4MaintenanceHigh-pr

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭3Sample degasserThe sample degasser removes gas bubbles an

1.3 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)1.3 Safety instructions1.3.1 General notes on

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭5Protection against electrostatic chargesWARNINGElectronic

1.4 Symbols and conventions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)More details about the disposal of your old

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭72 Overview of the instrument2.1 FrontFigu

2.2 Rear￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)13Peristaltic pump14Metrohm CO2 Suppressor (MCS)15Detector cham

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭95Drainage tubing connectionFor connecting t

2.3 Feed-throughs for capillaries and cables￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)2.3 Feed-throughs for cap

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭11Openings on the back panelFigure 4 Opening

2.3 Feed-throughs for capillaries and cables￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Figure 5 Ducts for capilla

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭133 Installation3.1 Setting up the instrument3.1.1 Pack

3.2 Capillary connections in the IC system￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Also see: PEEK pressure scre

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭15￭ The capillary ends do not have exactly flat edges.￭ Th

3.3 Removing transport locking screws￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)3.3 Removing transport locking s

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭17CAUTIONThe pumps may be damaged if you transport the ins

3.4 Connecting the drainage tubing and leak sensor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Connecting the drain

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭19Route the loose end into a waste container.3.4.2 Connec

Metrohm AGCH-9100 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] Compact IC Flex930 Compact IC Flex Ov

3.6 Connecting the eluent bottle￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)3.6 Connecting the eluent bottleThe e

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭21 2Mounting the tubing adapter and the aspiration filterI

3.6 Connecting the eluent bottle￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560) 4Mounting the adsorber tubeNOTEDepend

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭233.7 Connecting the eluent degasserThe high-pressure pum

3.9 Installing an inline filter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Figure 9 High-pressure pump with purge

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭25Figure 10 Inline filter1Input capillaryConnected to the

3.11 Injection valve￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)The pulsation absorber is completely connected. No

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭27Figure 12 Exchanging the sample loop1Pressure screwFaste

3.12 Suppressor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)3.12 SuppressorThe suppressor drive of the 930 Compact

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭29CAUTIONThe rotor may be destroyed during start-up if not

TeachwareMetrohm AGCH-9100 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

3.12 Suppressor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)NOTEThe rotor's sealing surface is approximately 4

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭31￭ Insert the rotor into the adapter so that the tubing c

3.12 Suppressor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Recommended installationAlternative installationInstall

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭333.12.2.1 Installing the eluent pathThe eluent path is c

3.12 Suppressor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560) 1Prepare a tubing cartridge of the peristaltic pump fo

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭35Connecting the rinsing solution inlet to the peristaltic

3.13 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Order num-berName Material Inner diame-terUse6.18

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭37Pump tubing Adapter6.1826.390 (yellow/yellow)6.1826.420

3.13 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Installing the pump tubingFor this step you need

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭39￭ Install the pump tubing connection with safety device

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 Instrument de

3.13 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Setting the contact pressure correctly 1￭ Fully l

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭41Figure 14 Peristaltic pump1Contact pressure lever2Tubing

3.14 Metrohm CO2 Suppressor (MCS)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)ymer membrane. At the same time, the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭43 3Connection to the detectorConnect the detector input c

3.14 Metrohm CO2 Suppressor (MCS)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560) 1Preparing the adsorption cartridge

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭453.15 Installing the detectorThe 930 Compact IC Flex pro

3.16 Connecting the sample degasser (optional)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭46￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Connecting the sample de

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭473.17 Connecting the instrument to a computerNOTEThe ins

3.18 Connecting the instrument to the power supply￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭48￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)3.18 Connecting the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭49After being switched on, the LED on the front of the ins

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)3.13 Peristaltic pump ...

3.19 Initial start-up￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭50￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)MagIC Net detects the instrument and all of its m

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭51 5Setting the contact pressure of the peristaltic pump￭

3.20 Connecting and rinsing the guard column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭52￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)NOTEThe guard column may n

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭53￭ Optional: In case the guard column is connected to the

3.21 Connecting the separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭54￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)CAUTIONNew separation columns are

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭55Connecting the separation column 1Removing the stoppersC

3.21 Connecting the separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭56￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560) 2Installing the input of the sep

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭573.22 ConditioningAfter installation, after each time th

3.22 Conditioning￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭58￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭ Visually inspect whether all capillaries and their

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭594 OperationThe 930 Compact IC Flex Oven/SeS/PP/Deg is oper

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭V5.13 Peristaltic pump ...

5.1 IC system￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭60￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)5 Operation and maintenance5.1 IC system5.1.1 Operatio

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭615.1.4 Shutting down and starting back upIf

5.2 Capillary connections￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭62￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)5.2 Capillary connectionsAll connections bet

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭6312234Figure 16 Column oven1Column holderFor

5.5 Handling the eluent￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭64￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Replacing the preheating capillariesIn order to

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭65The composition of the eluent plays a criti

5.7 Notes on operating the high-pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭66￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Connecting the connecting

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭675.8 Servicing the high-pressure pumpFigure

5.8 Servicing the high-pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭68￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)CAUTIONMaintenance work on the hig

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭69Cleaning the outlet valve 1Removing the out

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VI￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)9 Accessories 111Index 113

5.8 Servicing the high-pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭70￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)NOTEThe maximum treatment time in

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭71Spare parts If the inlet valve cannot be cl

5.8 Servicing the high-pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭72￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)NOTEThe maximum treatment time in

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭73￭ Has the pressure dissipated?￭ Is the inst

5.8 Servicing the high-pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭74￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Figure 18 High-pressure pump – cro

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭7521Figure 19 Tool for piston seal (6.2617.01

5.8 Servicing the high-pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭76￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560) 3Removing the old piston sealCAUT

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭77Optional: Cleaning/replacing the zirconium

5.8 Servicing the high-pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭78￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Figure 22 Components of the piston

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭79You can find these parts in the accessory k

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of figures930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭VIITable of figuresFigure 1 Front ...

5.9 Servicing the inline filter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭80￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Connecting the input for the high-press

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭81Removing the filterFigure 23 Inline filter

5.9 Servicing the inline filter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭82￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)Inserting a new filter 1Inserting a new

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭835.10 Servicing the pulsation absorberCAUTI

5.12 Suppressor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭84￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)CAUTIONThe suppressor has to be regenerated (see Chapte

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭855.12.3.2 Regenerating the suppression roto

5.12 Suppressor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭86￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭ In the software, use the Step command to switch to th

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭87 2Dismantling the suppressor￭ Unscrew union

5.12 Suppressor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭88￭￭￭￭￭￭￭￭930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭ Insert the rotor (24-3) into the housing (24-4) in su

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)￭￭￭￭￭￭￭￭89Replacing parts of the suppressor 1Disconne