Metrohm 882 Compact IC plus – Anion – MCS User Manual

882 Compact IC plus882 Compact IC plus – Anion – MCSManual8.882.8013EN

5.14 Quality Management and validation with Metrohm￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭90￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSNoteYou can find information on th

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭916 Troubleshooting6.1 Problems and their solutionsProblem Cause Rem

6.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭92￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSProblem Cause RemedyMCS – not connected. Connect the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭93Problem Cause RemedyData of the separa-tion column cannotbe read.Col

6.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭94￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSProblem Cause RemedySeparation column – deadvolume at

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭957 Technical specifications7.1 Reference conditionsThe tec

7.5 Housing￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭96￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS7.5 HousingDimensionsWidth 302 mmHeight 562 mmDepth 368 mmMaterial of bas

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭97￭ The pump is automatically shut down at the first piston s

7.10 Metrohm CO2 Suppressor (MCS)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭98￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS7.10 Metrohm CO2 Suppressor (MCS)Material fluoropol

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭99Leak sensor 1 jack plugFurther connec-tionsAuxiliary 1 DSUB

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭11 Introduction1.1 Instrument descriptionThe instrument 882 Compact IC

7.15 Weight￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭100￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS7.15 WeightWeight 19.7 kg (without accessories)

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭1018 Conformity and warranty8.1 Declaration of ConformityThi

8.2 Quality Management Principles￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭102￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSThis instrument meets the requirements of the ETL L

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭103Software developmentSoftware development occurs in terms of

8.3 Warranty (guarantee)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭104￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSFaults arising from circumstances that are not the responsib

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭1059 AccessoriesNoteSubject to change without notice!9.1 Scope of delive

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭106￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSQty. Order no. Description2 6.1608.020 Glass bottle / 1000 mL /

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭107Qty. Order no. Description1 6.1803.040 PTFE capillary 0.5 mm i.d. / 1 m

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭108￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSQty. Order no. Description2 6.1816.020 Silicone tubing 6 mm i.d

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭109Qty. Order no. Description1 6.2151.020 Cable USB A - USB B / 1.8 mUSB c

1.2 About the documentation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSPulsation absorberThe pulsation absorber protects the separ

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭110￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSQty. Order no. Description1 6.2621.030 Hexagon key 4 mmLength (

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭111Qty. Order no. Description1 6.2621.100 Hexagon key 3 mmHexagon key 3 mm

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭112￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSQty. Order no. Description1 6.2744.014 Pressure screw 2xWith UN

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭113Qty. Order no. Description2 6.2744.070 Pressure screw shortShort versio

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭114￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSQty. Order no. Description1 6.2816.020 Syringe 10 mL with Luer

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭115Qty. Order no. Description1 6.2837.000 CO2 adsorption cartridgeAdsorpti

9.2 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭116￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSOrder no. Description6.2617.040 Tool for piston seal MacroFo

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭117Order no. Descriptionwell as GLP. Dialog languages: German, English, Fr

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭118￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSIndexNumbers/Symbols6.2821.090 aspiration filter ... 63(6.2821.130) Filter .

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Index882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭119Separation column ... 54Suppressor ... 45Instru

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭31.2.1 Symbols and conventionsThe following symbols and styles are used

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭120￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSTubingsInstallation ... 17UUSB ...

1.3 Intended use￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS1.3 Intended useThe instrument 882 Compact IC plus – Anion – MCS is u

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭5WarningOnly personnel qualified by Metrohm are authorized to carry out s

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS1.4.3 Tubing and capillary connectionsCautionLeaks in tubing a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭72 Overview of the instrument2.1 Front1234567891011Figure

2.2 Rear￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS2.2 Rear211201181719151412111098137654311216TypeMade by Metrohm Herisau Switz

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭9I = OnO = Off3Mains connection socketFor connecting the ma

3.1 About this chapter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS3 Installation3.1 About this chapterThe Installation chapter

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭11￭ Connect the leak sensor (see Chapter 3.6.2, page 20).￭ Connect the dr

3.2 Initial installation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS￭ Prepare a pump tubing for the rinsing solution:– Plug a tub

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭13 8Connecting the instrument￭ Connect the instrument to a computer on wh

3.3 Installation diagram￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS3.3 Installation diagramThe following installation diagram s

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭1512618181778910111213143418192018165152122Figure 3 Installation diagram

3.3 Installation diagram￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS3MSM eluent input capillaryLabeled with in.4MSM eluent output

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭173.4 Setting up the instrument3.4.1 PackagingThe instrument is supplie

3.5 Capillary connections in the IC system￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSPressure screws412 3Figure 4 Connection of

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭19￭ PEEK capillaries (6.1831.030) with an internal diameter of 0.75 mm fo

Metrohm AGCH-9100 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] Compact IC plus882 Compact IC plus –

3.6 Installations on the rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSColored sleeves for PEEK capillariesTh

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭21Connecting the leak sensorConnect the leak sensor as follows: 1Pull out

3.6 Installations on the rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS245613798Figure 6 Drainage tubings1Dra

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭23Installing drainage tubingsProceed as follows to install the drainage t

3.7 Capillary and cable feed-throughs￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS1231236745Figure 7 Capillary and cable feed-thro

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭253.8 Eluent3.8.1 Connecting eluent bottleThe eluent is aspirated out o

3.8 Eluent￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS1 234Figure 8 Installing eluent bottle attachment1Eluent aspiration tubing

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭27 4Install tubing weighting and aspiration filter1 2345Figure 10 Install

3.8 Eluent￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS￭ Fasten the completely equipped bottle attachment (10-2) on theeluent bott

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭293Cotton4CO2 adsorberAdsorbs CO2 from the air (e.g. Merck sodalime with

TeachwareMetrohm AGCH-9100 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

3.9 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS10891234562722211212213Figure 13 Capillary connections high pre

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭31NoteThe eluent aspiration capillary is already installed in the newly d

3.9 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS3.9.2 Deaerating the high pressure pumpThe high pressure pump

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭33Deaerate the high pressure pumpThe instrument must be connected to the

3.10 Inline filter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS 4Setting the flow rate￭ Start MagIC Net™ (if not yet started).￭ En

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭35Installing the inline filterCautionObserve the flow direction marked on

3.12 Injection valve￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSThe pulsation absorber protects the separation column from damage

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭37NoteThe capillaries of the eluent path and the sample path and the samp

3.12 Injection valve￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS 2Mounting new sample loop￭ Fasten one end of the sample loop (18

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭39Position B In the position INJECT, the eluent flows throughthe sample l

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 Instrument description ...

3.13 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS6143257Figure 20 Peristaltic pump1Knurled screw in the mounting

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭413.13.2 Installing the peristaltic pump6.2744.16016.2744.1802 3 4 5 6 7

3.13 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS 3Connecting the pressure sideNoteDepending on the use of the pe

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭43123Figure 23 Install pump tubing connection without filter1Union nut2Ad

3.13 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSPump tubing Adapter6.1826.340 (black/black)6.1826.360 (white/whi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭453.14 Metrohm Suppressor Module (MSM)The MSM is used for chemical suppr

3.14 Metrohm Suppressor Module (MSM)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭46￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS13234567821Figure 24 Suppressor – connection capi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭47Connect the PTFE capillaries firmly mounted on the connecting piece tot

3.15 Metrohm CO2 Suppressor (MCS)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭48￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS 4Connecting the rinsing the solution outlet capilla

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭491234 45 567Figure 25 MCS – connection1MCS inputConnection to the MSM.2M

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS3.12 Injection valve ...

3.15 Metrohm CO2 Suppressor (MCS)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭50￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS3.15.3 Installing the adsorption cartridgesFor effe

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭517H2O adsorption cartridge (6.2837.010)For removing the H2O from the asp

3.16 Connecting the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭52￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS3.16 Connecting the instrument3.16.1 Connecting the i

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭533.17 Guard columnThe use of guard columns serves for protecting the se

3.18 Separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭54￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSConnecting and rinsing the guard column 1Connecting the guard c

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭55CautionNew separation columns are filled with solution and are sealed o

3.18 Separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭56￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS 2Rinsing the separation column￭ Place beaker under the outlet

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Start-up882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭574 Start-upThe chapter Start-up is divided into 2 sections:Initial start-up

4.2 Conditioning￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭58￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS 4Deaerate the high pressure pump￭ Deaerate the high pressure pump(s)

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Start-up882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭59￭ Select (or create) a suitable method. 2Preparing the instrument￭ Ensure t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭V5.8 Inline sample preparation ...

5.1 General notes￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭60￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS5 Operation and maintenance5.1 General notes5.1.1 CareWarningThe

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭615.1.3 OperationCautionIn order to avoid disturbing temper

5.3 Door￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭62￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS5.3 DoorCautionThe door is made of PMMA (polymethylmetacrylate). It must nev

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭635.4.2 Operation5.4.2.1 Supply bottleThe supply bottle wi

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭64￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSCautionIn order to spare the pump seals, the pump should not be

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭65Cleaning/replacing the zirconium oxide pistonClean one pis

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭66￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS￭ Remove the backup ring from the pump head and lay to the othe

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭67for removing the old piston seal and a sleeve for insertin

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭68￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS12Figure 30 Removing the piston seal1Piston seal2Tool for pisto

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭6912Figure 32 Inserting the piston seal into the pump head 4

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VI￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS8 Conformity and warranty 1018.1 Declaration of Conformity ...

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭70￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS1234Figure 33 Removing valves1Outlet valve holder2Outlet valveO

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭71￭ Place the valve with the seal faced downwards above the

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭72￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS123567891098710546Figure 35 Components of the inlet valve and o

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭73￭ Place over the valve housing and hold it tightly.￭ By ti

5.6 Inline filter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭74￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSMounting the pump headNoteTo prevent the pump head from being positi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭75Changing the filterThe flow must be stopped before changin

5.7 Injection valve￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭76￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS5.7 Injection valve 5.7.1 ProtectionTo prevent contamination of

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭77 2Aspirating the sample and measuring timeAspirate a sampl

5.10 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭78￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS5.10 Peristaltic pump5.10.1 OperationThe pumping capacity of t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭79Table 2 Pump tubingOrdernumberName Material InnerdiameterU

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of figures882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭VIITable of figuresFigure 1 Front 882 Compact IC plus – Anion – MCS ...

5.11 Metrohm Suppressor Module (MSM)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭80￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS123Figure 37 Pump tubing connection – Changing th

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭815.11.2 Operation Suppressor NoteThe suppressor units must

5.11 Metrohm Suppressor Module (MSM)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭82￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS5.11.3 Maintenance5.11.3.1 Parts of the suppres

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭83Regenerating the suppressor 1Disconnecting the suppressor

5.11 Metrohm Suppressor Module (MSM)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭84￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS5.11.3.3 Cleaning the suppressor In the followin

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭85 5Inserting the rotorCautionAn incorrectly inserted rotor

5.11 Metrohm Suppressor Module (MSM)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭86￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCSReplacing parts of the suppressorReplace the part

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭87 6Inserting the new connecting piece￭ Insert the connectin

5.13 Separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭88￭￭￭￭￭￭￭￭882 Compact IC plus – Anion – MCS1Allow material to dry loose (not in cartridge) at 140 °C overn

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance882 Compact IC plus – Anion – MCS￭￭￭￭￭￭￭￭895.13.3 StorageAlways store the separation columns sealed