Metrohm 870 KF Titrino plus Installation User Manual

870 KF Titrino plusInstallation and tutorial8.870.8004EN

2.1 Setting up and connecting the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭870 KF Titrino plusConnecting the titration stand to the MSB 1Observe the m

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Installation870 KF Titrino plus￭￭￭￭￭￭￭￭5Connecting a balanceBalances are equipped as a rule with a serial RS 232 interface. To

2.2 Setting up the KF titration cell￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭870 KF Titrino plus2.2 Setting up the KF titration cellMounting the KF titration c

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Installation870 KF Titrino plus￭￭￭￭￭￭￭￭7 4Adjust the height of the KF titration cell by pressing the locking lever.It should a

2.2 Setting up the KF titration cell￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭870 KF Titrino plusEquipping the KF titration cell6.2730.0206.2730.0106.0338.1006.1

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Installation870 KF Titrino plus￭￭￭￭￭￭￭￭92.3 Setting up the aspiration and solvent bottleMode of operation of the 803 Ti Stand

2.3 Setting up the aspiration and solvent bottle￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭870 KF Titrino plusMetrohm offers suitable thread adapters for bottles

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Installation870 KF Titrino plus￭￭￭￭￭￭￭￭11 7Place the completely equipped bottle top 6.1602.105 on the amberglass bottle 6.1608

2.4 Connecting the pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭870 KF Titrino plus 3Place the bottle top on the clear glass bottle 6.1608.030 (or on a dif-fer

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Installation870 KF Titrino plus￭￭￭￭￭￭￭￭132.5 Setting up tubings and tipsSetting up the aspiration and dosing tip123456.2730.0

2.5 Setting up tubings and tips￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭870 KF Titrino plusAttaching the exchange unit 1Slide the exchange unit from the front

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭153 Tutorial3.1 ConfigurationNoteExternal devices (printer, balance and USB stick) must b

3.1 Configuration￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭870 KF Titrino plusSwitching off the instrumentProceed as follows: 1￭ Keep the red [STOP] key pressed

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭17The solutions are configured under System ▶ Solutions.Proceed as follows: 1Open the solut

3.1 Configuration￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭870 KF Titrino plus 2Define a name￭ With the arrow keys [⇦] or [⇨], select the function Edit in thefu

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭19￭ Enter the theoretical concentration of the titrant and apply withAccept or [BACK].The i

3.1 Configuration￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭870 KF Titrino plus￭ Select the menu item System and open the system dialog with[OK].￭ Select the men

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭21Selecting a printerIf you would like to print the results automatically or manually, you

3.2 Carrying out titrations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭870 KF Titrino plus￭ Select the a balance type and apply with [BACK].The balance is entered

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭23￭ In the main dialog, select Method and confirm with [OK].The method table with the store

Metrohm AGCH-9101 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] KF Titrino plusInstallation and tutor

3.2 Carrying out titrations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭870 KF Titrino plus￭ Select the parameter Solution and confirm with [OK].The list of the co

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭25￭ Select the menu item Statistics and open the corresponding dia-log with [OK].￭ Select t

3.2 Carrying out titrations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭870 KF Titrino plus￭ Select on and confirm with [OK]. 6Save the method￭ The modified parame

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭27￭ With the arrow keys [⇦] or [⇨], select the function PREP in thefunction bar and confirm

3.2 Carrying out titrations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭870 KF Titrino plus 2Inject water standardNoteCalculate the amount of the water standard in

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭29The titration starts and the curve is displayed:After the completion of the titration, th

3.2 Carrying out titrations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭870 KF Titrino plusThe result and the sample size of each determination are shown. On/Off r

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭31 2Select a solution￭ In the main dialog, select Menu and confirm with [OK].The main menu

3.2 Carrying out titrations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭870 KF Titrino plus￭ Select the menu item Calculation and open the correspondingdialog with

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭33NoteContinue with step 6, if you do not have a printer connected. 5Select the reports￭ Wi

TeachwareMetrohm AGCH-9101 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

3.2 Carrying out titrations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭870 KF Titrino plus3.2.5 Determining the water content of a sampleYou can use either the w

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭35 2Enter the sample dataYou can enter information about the sample in different ways. Youc

3.2 Carrying out titrations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭870 KF Titrino plus￭ Press [START].Conditioning is stopped. The request for adding the samp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Tutorial870 KF Titrino plus￭￭￭￭￭￭￭￭37 6Carry out the remaining determinations￭ Carry out the remaining titer determinations in

3.2 Carrying out titrations￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭870 KF Titrino plus 8Cancel the conditioning￭ Press [STOP].Conditioning is canceled and the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents870 KF Titrino plus￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 Structure of the tutorial ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction870 KF Titrino plus￭￭￭￭￭￭￭￭11 Introduction1.1 Structure of the tutorialThis tutorial describes the installation

2.1 Setting up and connecting the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭870 KF Titrino plus2 Installation2.1 Setting up and connecting the instru

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Installation870 KF Titrino plus￭￭￭￭￭￭￭￭3Mounting the stand11236.2016.0706.2001.060 1Screw the stand plate 6.2001.060 with the