Metrohm 860 KF Thermoprep User Manual

860 KF ThermoprepManual8.860.8003EN

1.2 About the documentation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭860 KF Thermoprep1.1.2 Intended useThe 860 KF Thermoprep is designed for usage as an auxili

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction860 KF Thermoprep￭￭￭￭￭￭￭￭3WarningThis symbol draws attention to a possible hazard dueto heat or hot instrument par

1.3 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭860 KF ThermoprepWarningNever open the housing of the instrument. The instrument could bedamaged

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction860 KF Thermoprep￭￭￭￭￭￭￭￭5WarningThere is a considerable risk of injury connected with the needles.Grasp the handl

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭860 KF Thermoprep2 Overview of the instrument12345678910111213Figure 1 Front 860 KF Thermoprep1Guide head2Needle holde

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument860 KF Thermoprep￭￭￭￭￭￭￭￭718235 674Figure 2 Rear 860 KF Thermoprep1Air pump inletWith 6.2724.010 dus

3.1 Setting up the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭860 KF Thermoprep3 Installation3.1 Setting up the instrument3.1.1 PackagingThe instrume

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation860 KF Thermoprep￭￭￭￭￭￭￭￭93.3 Mounting the guidance rodThe guidance rod with the guide head is enclosed separatel

3.3 Mounting the guidance rod￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭860 KF Thermoprep45Figure 5 Mounting the guidance rod 5Insert the guidance rod into the o

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation860 KF Thermoprep￭￭￭￭￭￭￭￭111089Figure 7 Fix the adapter 9Fix the adapter in the guidance rod. Fasten the screw in

3.4 Mounting the sample insert￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭860 KF Thermoprep3.4 Mounting the sample insert6.2063.0106.2627.000Figure 9 Mounting th

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation860 KF Thermoprep￭￭￭￭￭￭￭￭133.5 Mounting the needlesThe length of the needle holder defines how deeply the injecti

3.6 Mounting the heating tubing￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭860 KF Thermoprep 2Screw the 6.2816.080 outlet needle onto the Luer connector ofthe nee

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation860 KF Thermoprep￭￭￭￭￭￭￭￭15 2Use the accompanying knurled screw to screw the 6.2060.010cable holder tightly onto t

3.7 Mounting the dust filter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭860 KF Thermoprep3.7 Mounting the dust filterThe built-in air pump must be protected agai

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation860 KF Thermoprep￭￭￭￭￭￭￭￭17 2Screw one 6.1821.040 filter tube into each of the 6.1602.145drying flask covers from

3.9 Air/nitrogen connector￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭860 KF Thermoprep 3Screw the second 6.1805.080 FEP tubing (25 cm length) to the gasinlet (at

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation860 KF Thermoprep￭￭￭￭￭￭￭￭193.10 Inserting the heating tube into the KF titration cellThe 860 KF Thermoprep can be

3.10 Inserting the heating tube into the KF titration cell￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭860 KF Thermoprep 5Shift the tip vertically in such a way th

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation860 KF Thermoprep￭￭￭￭￭￭￭￭21 5Shift the height of the tip of the heating tube vertically in such a waythat the outl

Metrohm AGCH-9101 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] KF ThermoprepManual8.860.8003EN 07/20

4.1 Switching the instrument on and off￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭860 KF Thermoprep4 Operation4.1 Switching the instrument on and offThe rocker

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation860 KF Thermoprep￭￭￭￭￭￭￭￭23[◀]Reduces gas flow by 1 mL/min during ongoing opera-tion. Keep the key pressed down brief

4.3 The display￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭860 KF ThermoprepSymbol SignificanceAn error has occurred. The type of the error will be iden-tified in

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation860 KF Thermoprep￭￭￭￭￭￭￭￭254.4 Modifying numerical values and settingsThe instrument settings can be modified in two

4.5 Parameters￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭860 KF Thermoprep4.5 Parameters[OK]The instrument parameters can be adjusted in a menu that is opened b

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Operation860 KF Thermoprep￭￭￭￭￭￭￭￭27Only when 'gas type' = 'other'.Range0.001 ... 2.000 (Increment: 0.001

4.6 Configuration￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭860 KF Thermoprepin addition to switching the gas flow on and off. Furthermore it is still pos-sible

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Performing a determination860 KF Thermoprep￭￭￭￭￭￭￭￭295 Performing a determinationMoisture determinations according to the hea

5.1 Conditioning the system￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭860 KF ThermoprepIt is advantageous to have air bubbles stirred into the workingmedium and

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Performing a determination860 KF Thermoprep￭￭￭￭￭￭￭￭31Figure 22 Insert the sample vessel into the ovenInserting the needle 1Gri

TeachwareMetrohm AGCH-9101 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

5.1 Conditioning the system￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭860 KF ThermoprepFigure 24 Insert the needleSwitching on the gas flow 1Press the [OK] key a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Performing a determination860 KF Thermoprep￭￭￭￭￭￭￭￭33NoteThe signal drift on the KF titrator should be less than 20 µg/min (or

5.3 Determining samples￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭860 KF ThermoprepNoteCaution! The vessel is hot. 4Place the blank into the oven using the crimp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Performing a determination860 KF Thermoprep￭￭￭￭￭￭￭￭35Starting the sample determination 1Start the determination by pressing th

6.1 General￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭860 KF Thermoprep6 Handling and maintenance6.1 GeneralThe 860 KF Thermoprep requires appropriate care. Ex

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Handling and maintenance860 KF Thermoprep￭￭￭￭￭￭￭￭37addition, various application bulletins are also available on the subject,w

7.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭860 KF Thermoprep7 Troubleshooting7.1 Problems and their solutionsProblem Cause Reme

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Appendix860 KF Thermoprep￭￭￭￭￭￭￭￭398 Appendix8.1 Practical instructionsCarrier gas selectionIf the hot sample is sensitive t

8.2 Literature￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭860 KF Thermoprep8.2 Literature￭ E. Scholz, Hydranal®-Manual, Riedel-de Haën, 1996￭ P. Bruttel, R. Schl

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Technical data860 KF Thermoprep￭￭￭￭￭￭￭￭419 Technical data9.1 OvenTemperaturerange50…250 °CAccuracy±3 °CCorrection range-10…+

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents860 KF Thermoprep￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 Instrument description ...

9.4 Mains connection￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭860 KF Thermoprep9.4 Mains connectionVoltage100…120 / 220…240 VFrequency50 / 60 HzPower consump-t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Technical data860 KF Thermoprep￭￭￭￭￭￭￭￭439.7 Ambient temperatureNominal functionrange5…45 °CHumidity < 80 %Storage–20…70 °

10.1 Declaration of Conformity￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭860 KF Thermoprep10 Conformity and warranty10.1 Declaration of ConformityThis is to cer

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10 Conformity and warranty860 KF Thermoprep￭￭￭￭￭￭￭￭45EN 61010-2-010 Particular requirements for laboratory equipmentfor the heat

10.3 Quality Management Principles￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭46￭￭￭￭￭￭￭￭860 KF Thermoprep10.3 Quality Management PrinciplesMetrohm Ltd. holds the ISO 9001:

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10 Conformity and warranty860 KF Thermoprep￭￭￭￭￭￭￭￭47tional Qualification and Performance Verification of the system compo-nents

11.1 Scope of delivery 2.860.0010￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭48￭￭￭￭￭￭￭￭860 KF Thermoprep11 AccessoriesNoteSubject to change without notice.11.1 Scope of de

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭11 Accessories860 KF Thermoprep￭￭￭￭￭￭￭￭49Qty. Order no. Description2 6.1608.050 Drying bottle / 100 mL / GL 45Material: Clear gl

11.1 Scope of delivery 2.860.0010￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭50￭￭￭￭￭￭￭￭860 KF ThermoprepQty. Order no. Description1 6.1805.100 FEP tubing / M6 / 40 cmWith l

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭11 Accessories860 KF Thermoprep￭￭￭￭￭￭￭￭51Qty. Order no. Description2 6.1821.040 Filter tubeFilter tube for 6.1608.050 Drying bot

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭860 KF Thermoprep4.4 Modifying numerical values and settings ... 254.4.1 Select

11.1 Scope of delivery 2.860.0010￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭52￭￭￭￭￭￭￭￭860 KF ThermoprepQty. Order no. Description1 6.2060.010 Cable supportUsed with 860 KF

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭11 Accessories860 KF Thermoprep￭￭￭￭￭￭￭￭53Qty. Order no. Description1 6.2621.120 Hexagon key 1.5 mm1 6.2621.130 Hexagon key 2 mm1

11.1 Scope of delivery 2.860.0010￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭54￭￭￭￭￭￭￭￭860 KF ThermoprepQty. Order no. Description1 6.2739.000 WrenchFor tightening connecto

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭11 Accessories860 KF Thermoprep￭￭￭￭￭￭￭￭55Qty. Order no. DescriptionCable plug according to customer requirements.Switzerland: Ty

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭56￭￭￭￭￭￭￭￭860 KF ThermoprepIndexNumbers/Symbols6.2627.000 oven insert ... 12AArrow key ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents860 KF Thermoprep￭￭￭￭￭￭￭￭V10.3 Quality Management Principles ... 4611 Acce

Table of figures￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VI￭￭￭￭￭￭￭￭860 KF ThermoprepTable of figuresFigure 1 Front 860 KF Thermoprep ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction860 KF Thermoprep￭￭￭￭￭￭￭￭11 Introduction1.1 Instrument descriptionThe 860 KF Thermoprep is used whenever the hea